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Table 10 DSC values by layer from PEEK_50NdFeB prints. (Tg glass transition temperature, Xm Melting peak Crystallinity, Tm Melting temperature; the index I and II indicates the first and second heating cycle, the subscript CC indicates the cold crystallization)

From: 3D printing of high performance polymer-bonded PEEK-NdFeB magnetic composite materials

 

Tg I [°C]

Xm I [%]

Tm I [°C]

Xcc[%]

Tcc[°C]

Tg II [°C]

Xm II [%]

TmII [°C]

Top layer

149.0

30.8

340.2

–

–

139.9

38.6

332.0

Mid layer

145.2

30.4

339.1

–

–

140.0

38.5

337.7

Bottom layer

142.7

7.9

338.5

22.2

171.4

141.2

34.6

337.3